Desenvolvimento de processos avançados e sustentáveis para extração e análise de polifenóis em amostras de própolis

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Contieri, Letícia Sanches; Rostagno, Maurício Ariel, 2025, "Desenvolvimento de processos avançados e sustentáveis para extração e análise de polifenóis em amostras de própolis", https://doi.org/10.25824/redu/N95RME, Repositório de Dados de Pesquisa da Unicamp, V1, UNF:6:kfWweoRKYRcaSLHB1/oL2w== [fileUNF]

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Description	The data present spreadsheets, tables and chromatograms related to the research data presented in the "related publications". Where they are presented development of alternative and sustainable processes for extraction and analysis of polyphenols in propolis samples, focusing on the green (Brazilian) and yellow (Portuguese) varieties, Among the data presented, the following stand out: the creation and application of an innovative and universal analysis method for propolis extracts, based on the UHPLC-PDA (Ultra High Performance Liquid Chromatography - Photo Diode Array) chromatographic system; the development and application of a new extraction solvent (Betaine: Citric Acid 1:2) as an alternative to ethanol; the development of a new extraction and analysis platform coupled in lines through the PLE-PDA (Pressurized Liquid Extraction - Photo Diode Array) system; and the creation of a new metric, Path2Green, to assess the sustainability of extraction processes from biomass and the production of a propolis-based biomembrane. (2025-04-27)
Subject	Agricultural Sciences; Chemistry; Earth and Environmental Sciences; Medicine, Health and Life Sciences
Keyword	Propolis, Extraction, Sustaintability
Related Publication	CONTIERI, Leticia S. et al. Recent progress on the recovery of bioactive compounds obtained from propolis as a natural resource: Processes, and applications. Separation and Purification Technology, v. 298, p. 121640, 2022. doi: https://doi.org/10.1016/j.seppur.2022.121640
License/Data Use Agreement	CC BY-NC 4.0

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	1 to 7 of 7 Files	Original Format Archival Format (.tab)
	Betaína ácido cítrico extração.tab Tabular Data - 4.4 KB Published May 27, 2025 0 Downloads 13 Variables, 33 Observations UNF:6:H5yC8CLTpw8SBWVGk/P6UA== Extração com betaína e ácido cítricio propolis	Access File ???file.accessBtn.header.access??? Public Download Options MS Excel Spreadsheet (Original File Format) Tab-Delimited RData ???file.accessBtn.header.metadata??? Variable Metadata Data File Citation EndNote XML RIS BibTeX
	Dados amostras comerciais propolis.tab Tabular Data - 26.8 KB Published May 27, 2025 1 Download 45 Variables, 105 Observations UNF:6:5WVyZr4q3FEjEq/v33qKxA== Análise de conteúdo fenólico referente a amostras comerciais de extratos de própolis. Análise realizada através do método UPLC-PDA (doi: 10.1002/jssc.202200440)	Access File ???file.accessBtn.header.access??? Public Download Options MS Excel Spreadsheet (Original File Format) Tab-Delimited RData ???file.accessBtn.header.metadata??? Variable Metadata Data File Citation EndNote XML RIS BibTeX
	Dados injeções UPLC propolis.tab Tabular Data - 9.1 KB Published May 27, 2025 1 Download 20 Variables, 50 Observations UNF:6:yXycmSO6FyeIoMA8dXpfrA== Dados brutos extratos controle de própolis após injetados no sistema UPLC-PDA (referência:10.1002/jssc.202200440)	Access File ???file.accessBtn.header.access??? Public Download Options MS Excel Spreadsheet (Original File Format) Tab-Delimited RData ???file.accessBtn.header.metadata??? Variable Metadata Data File Citation EndNote XML RIS BibTeX
	Efeito dos solventes de extração propolis.tab Tabular Data - 3.2 KB Published May 27, 2025 0 Downloads 47 Variables, 23 Observations UNF:6:LTOFaJbY2AITzIV/bfIzyg== Efeito dos solventes de extração própolis	Access File ???file.accessBtn.header.access??? Public Download Options MS Excel Spreadsheet (Original File Format) Tab-Delimited RData ???file.accessBtn.header.metadata??? Variable Metadata Data File Citation EndNote XML RIS BibTeX
	Sólidos e oxidacao - amostras comerciais.tab Tabular Data - 9.3 KB Published May 27, 2025 0 Downloads 8 Variables, 90 Observations UNF:6:n8/EDXTavu1HgvWHDrudIw== Análises de sólidos totais e tempo de oxidação em extratos comerciais de própolis	Access File ???file.accessBtn.header.access??? Public Download Options MS Excel Spreadsheet (Original File Format) Tab-Delimited RData ???file.accessBtn.header.metadata??? Variable Metadata Data File Citation EndNote XML RIS BibTeX
	Temperatura sonda de US.tab Tabular Data - 254 B Published May 27, 2025 0 Downloads 22 Variables, 5 Observations UNF:6:OaF5ZQjDaNQDWFjJE7Dq8A== Efeito da temperatura de extração de fenólicos da própolis: sonda de ultrassom	Access File ???file.accessBtn.header.access??? Public Download Options MS Excel Spreadsheet (Original File Format) Tab-Delimited RData ???file.accessBtn.header.metadata??? Variable Metadata Data File Citation EndNote XML RIS BibTeX
	Testes bioadesão membrana.tab Tabular Data - 3.1 KB Published May 27, 2025 0 Downloads 19 Variables, 32 Observations UNF:6:rhYYoNPhjwrtmnzrkahl1Q== Teste de bioadesão das membranas carregadas com própolis + PLA	Access File ???file.accessBtn.header.access??? Public Download Options MS Excel Spreadsheet (Original File Format) Tab-Delimited RData ???file.accessBtn.header.metadata??? Variable Metadata Data File Citation EndNote XML RIS BibTeX

Citation Metadata

Persistent Identifier	doi:10.25824/redu/N95RME
Publication Date	2025-05-27
Title	Desenvolvimento de processos avançados e sustentáveis para extração e análise de polifenóis em amostras de própolis
Author	Contieri, Letícia Sanches (Universidade Estadual de Campinas (UNICAMP). Faculdade de Ciências Aplicadas) - ORCID: https://orcid.org/0000-0002-1439-5619 Rostagno, Maurício Ariel (Universidade Estadual de Campinas (UNICAMP). Faculdade de Ciências Aplicadas) - ORCID: https://orcid.org/0000-0003-1763-5697
Point of Contact	Use email button above to contact. Rostagno, Maurício Ariel (Universidade Estadual de Campinas (UNICAMP). Faculdade de Ciências Aplicadas)
Description	The data present spreadsheets, tables and chromatograms related to the research data presented in the "related publications". Where they are presented development of alternative and sustainable processes for extraction and analysis of polyphenols in propolis samples, focusing on the green (Brazilian) and yellow (Portuguese) varieties, Among the data presented, the following stand out: the creation and application of an innovative and universal analysis method for propolis extracts, based on the UHPLC-PDA (Ultra High Performance Liquid Chromatography - Photo Diode Array) chromatographic system; the development and application of a new extraction solvent (Betaine: Citric Acid 1:2) as an alternative to ethanol; the development of a new extraction and analysis platform coupled in lines through the PLE-PDA (Pressurized Liquid Extraction - Photo Diode Array) system; and the creation of a new metric, Path2Green, to assess the sustainability of extraction processes from biomass and the production of a propolis-based biomembrane. (2025-04-27)
Subject	Agricultural Sciences; Chemistry; Earth and Environmental Sciences; Medicine, Health and Life Sciences
Keyword	Propolis Extraction Sustaintability
Related Publication	CONTIERI, Leticia S. et al. Recent progress on the recovery of bioactive compounds obtained from propolis as a natural resource: Processes, and applications. Separation and Purification Technology, v. 298, p. 121640, 2022. doi: https://doi.org/10.1016/j.seppur.2022.121640 https://www.sciencedirect.com/science/article/pii/S1383586622011960?casa_token=5EjWtb0953EAAAAA:w2uMUE125hZQKwdXmdvmiwsPRGW9HAxULrgkg4gj8-SeIjcVCydHiQtp0Ech7cXf533CqjBSWzNH CONTIERI, Letícia S. et al. Ultra‐high‐performance liquid chromatography using a fused‐core particle column for fast analysis of propolis phenolic compounds. Journal of Separation Science, v. 46, n. 3, p. 2200440, 2023. doi: https://doi.org/10.1002/jssc.202200440 https://analyticalsciencejournals.onlinelibrary.wiley.com/doi/abs/10.1002/jssc.202200440?casa_token=fmAwb9hJdu4AAAAA%3A-c-ZKBpXZJmoPeTx77KYi_By56HlEY0acPBLabCzc35vWX-mGz3jq1frzVj7R35Gn1_yJgW_0DWdKNqk_Q CONTIERI, Letícia S. et al. Standardization proposal to quality control of propolis extracts commercialized in Brazil: A fingerprinting methodology using a UHPLC-PDA-MS/MS approach. Food Research International, v. 161, p. 111846, 2022. doi: https://doi.org/10.1016/j.foodres.2022.111846 https://www.sciencedirect.com/science/article/pii/S0963996922009048 CONTIERI, Letícia S. et al. Unlocking the full potential of green propolis: a novel extraction approach using eutectic solvents for improved phenolic compound recovery. ACS Sustainable Chemistry & Engineering, v. 11, n. 36, p. 13470-13482, 2023. doi: https://doi.org/10.1021/acssuschemeng.3c03812 https://pubs.acs.org/doi/full/10.1021/acssuschemeng.3c03812?casa_token=zbtM1rnFeXoAAAAA%3Awz9cKNyYOuxf5pIVyN2mOKFa8MTc2co9lUyMnqsihDF3fLXVD6nZx7qu2tYK45hJL3xEEPK4D0sbkUMyeA S CONTIERI, Letícia et al. Development of Poly (l-lactic acid)-Yellow Propolis Membranes for Antioxidant Applications. ACS Applied Polymer Materials, v. 6, n. 23, p. 14290-14299, 2024. doi: https://doi.org/10.1021/acsapm.4c01899 https://pubs.acs.org/doi/full/10.1021/acsapm.4c01899 S CONTIERI, Letícia et al. Sustainable and Innovative Method for Real-Time Extraction and Analysis of Polyphenols from Green Propolis by Pressurized Liquid Extraction Coupled Inline with Photodiode Array Detection (PLE-PDA). ACS Sustainable Chemistry & Engineering, v. 12, n. 52, p. 18735-18747, 2024. https://doi.org/10.1021/acssuschemeng.4c08602 https://pubs.acs.org/doi/full/10.1021/acssuschemeng.4c08602 DE SOUZA MESQUITA, Leonardo M. et al. Path2Green: introducing 12 green extraction principles and a novel metric for assessing sustainability in biomass valorization. Green Chemistry, v. 26, n. 19, p. 10087-10106, 2024. doi: DOI: 10.1039/D4GC02512A https://pubs.rsc.org/en/content/articlehtml/2024/gc/d4gc02512a
Funding Information	Fundação de Amparo à Pesquisa do Estado de São Paulo: FAPESP: 2020/03623-2 Fundação de Amparo à Pesquisa do Estado de São Paulo: FAPESP: 2021/11023-8
Depositor	Sanches Contieri, Letícia
Deposit Date	2025-03-27
Declarações obrigatórias sobre ética e privacidade	o projeto que gerou os dados foi aprovado pelo Comite de Ética em Pesquisa da Unicamp ou não envolve questões que requeiram tal aprovação; os dados que serão depositados estão de acordo com a LGPD (Lei Geral de Proteção de Dados)

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